AQA A Level & AS Level Chemistry - Required Core Practical Summary Notes (Methodology, Analysis, Results and Observations)
41 views 6 purchases
Course
Core Practicals
Institution
AQA
This document is a detailed and extensive guide for all of the 12 required practicals for AQA A level and AS Level chemistry. Revising the core practicals for exams can be difficult, so I prepared a resource which not only contains the method for each practical but also highlights where specific eq...
Required Chemistry Practicals
1. Make up a volumetric solution and carry out a simple acid–base titration
2. Measurement of an enthalpy change
3. Investigation of how the rate of a reaction changes with temperature
4. Carry out simple test-tube reactions to identify:
I. Cations – Group 2, NH4+
II. Anions – Group 7 (halide ions), OH–, CO32-, SO42-
5. Distillation of a product from a reaction
6. Tests for alcohol, aldehyde, alkene and carboxylic acid
7. Measuring the rate of reaction:
I. By an initial rate method
II. By a continuous monitoring method
8. Measuring the EMF of an electrochemical cell
9. Investigate how pH changes when a weak acid reacts with a strong base and when a
strong acid reacts with a weak base
10. Preparation of:
I. A pure organic solid and test of its purity
II. A pure organic liquid
11. Carry out simple test-tube reactions to identify transition metal ions in aqueous
solution
12. Separation of species by thin-layer chromatography
, 1. Making up a Volumetric Solution
Method
1) Calculate the mass of solid needed to produce 250cm3 of a 0.1 mol dm-3 solution.
2) Weigh the mass of an empty, clean weighing boat on a 2d.p. balance.
3) Add the calculated mass of solid into the weighing boat using a spatula and reweigh.
4) Pour the contents of the weighing boat into a 250cm3 beaker and reweigh.
The difference in mass is an accurate measurement of the mass of solid that is added to the beaker.
5) Add approx. 100cm3 of distilled water to the beaker and stir using a glass rod until all of the solid
dissolves.
It does not matter if the volume of water added slightly exceeds 100cm 3, as the volume must be made
up to 250cm3 in the end.
Substances may not dissolve well in cold water, in which case the contents could be heated gently.
6) Using a funnel, pour the contents of the beaker into a 250cm3 volumetric flask and rinse the glass rod
/ beaker contents into the flask.
Rinsing the glassware ensures that all of the salt is transferred into the volumetric flask.
7) Carefully add distilled water to the volumetric flask up to the graduated line.
Use a dropping pipette for the last few drops to ensure you don’t overshoot the graduated mark.
Fill until the bottom of the meniscus sits on the graduated line.
8) Stopper the flask.
A stopper will prevent water from evaporating from the flask. If water evaporated from the flask, the
concentration of the solution will increase.
9) Invert the flask to mix the contents.
Only invert the flask after reaching the graduated line, otherwise water will remain on the edges of
the flask and gradually add to the solution, reducing the concentration.
Inverting will ensure that the concentration of the substance is uniform throughout the solution.
Potential Sources of Error
• If using an anhydrous salt, make sure it has not picked up water otherwise its mass values will not be
accurate.
• Balance only gives values to 0.01g.
• With dark liquids, it can be difficult to see the meniscus – place a piece of white paper behind the
marker clearer to see.
Reducing Uncertainty in Measuring Mass
• Use a balance with a higher resolution.
• Use a larger mass of solid.
• Weigh the sample before and after the addition of the solid to the beaker (weigh by difference).
The benefits of buying summaries with Stuvia:
Guaranteed quality through customer reviews
Stuvia customers have reviewed more than 700,000 summaries. This how you know that you are buying the best documents.
Quick and easy check-out
You can quickly pay through credit card or Stuvia-credit for the summaries. There is no membership needed.
Focus on what matters
Your fellow students write the study notes themselves, which is why the documents are always reliable and up-to-date. This ensures you quickly get to the core!
Frequently asked questions
What do I get when I buy this document?
You get a PDF, available immediately after your purchase. The purchased document is accessible anytime, anywhere and indefinitely through your profile.
Satisfaction guarantee: how does it work?
Our satisfaction guarantee ensures that you always find a study document that suits you well. You fill out a form, and our customer service team takes care of the rest.
Who am I buying these notes from?
Stuvia is a marketplace, so you are not buying this document from us, but from seller JunaidAli025. Stuvia facilitates payment to the seller.
Will I be stuck with a subscription?
No, you only buy these notes for $9.82. You're not tied to anything after your purchase.
